化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → 1,1-Cyclohexanedicarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | Cyclohexane-1,1-dicarboxylic acid | HCID 136906 | — |
| 反応物 | 1,1-Cyclohexanedicarboxamide | HCID 299204 | — |
| 生成物 | 1,1-Cyclohexanedicarboxamide | HCID 299204 | — |
| 生成物 | 1,1-Cyclohexanedicarbonitrile | HCID 544561 | — |
反応手順
Furthermore, as a method for producing bis(aminomethyl)cyclohexane, for example, Non-Patent Document 1 (Malachowski et al.) discloses the following: an acid chloride derivative is prepared using cyclohexanedicarboxylic acid with thionyl chloride; cyclohexane diamide is prepared using the acid chloride derivative with ammonia; and thereafter, the cyclohexane diamide is further allowed to react with thionyl chloride to obtain dicyanocyclohexane, and then the obtained dicyanocyclohexane is hydrogenated.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08865938B2 |
| 出典データセット | uspto-grants-2014_10 |
| ORD ID | ord-17d89f5f75154560a35f326706e8dd50 |
| 出典メモ | uspto-grants-2014_10 |