化工社化工社 化学情報印刷レポート · 研究参考用
Ferulic Acid → Dihydroferulic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ferulic Acid | HCID 445858 | — |
| 触媒 | HCID 178418390 | HCID 178418390 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Dihydroferulic Acid | HCID 14340 | 95.5% |
反応手順
20.0 g of Ferulic acid was dissolved in 250 ml of methanol and subjected to catalytic reduction under normal pressure for 3 hours in the presence of 10% palladium carbon catalyst (50% wet type). After removing the catalyst by filtration, the resulting filtrate was concentrated to collect precipitated crystals by filtration, thereby obtaining 19.3 g of 3-(4-hydroxy-3-methoxyphenyl)propionic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05620991 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-82b17ac5b1d24f1eb4c9fd8d2d950180 |
| 出典メモ | uspto-grants-1997_04 |