Hydroxylamine → HCID 136346368、化合物
反応式
[Br:1][C:2]1[C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[C:5]([CH:12]=O)=[CH:4][CH:3]=1.[NH2:14][OH:15]>C(O)C>[Br:1][C:2]1[C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[C:5]([CH:12]=[N:14][OH:15])=[CH:4][CH:3]=1参加物
4
実験手順
To a stirred solution of 8-bromo-5-quinolinecarboxaldehyde (i.e. the product from Step B) (1.7 g, 7.1 mmol) in ethanol (30 mL) was added an aqueous solution of hydroxylamine (0.7 mL, 50% in water). After stirring at room temperature for 2 h, the reaction mixture was concentrated under reduced pressure to provide the title compound as a pale yellow solid (1.8 g).
後処理
- concentrationthe reaction mixture was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-3f22568a5e044c4aa6ed95f51dbedd86
- 出典データセット
- uspto-grants-2014_10
- 特許番号
- US08871941B2
反応ノート
読み込み中…