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HRID 542869作成日:2026年10月26日

Hydrochloric Acid → 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochloride

https://huagongshe.com/reaction/542869

反応式

関与物質

役割名称HCID仕込み量
反応物Hydrochloric AcidHCID 313—
反応物Diisopropyl EtherHCID 7914—
反応物3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazoleHCID 13054018—
溶媒EthanolHCID 702—
生成物3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochlorideHCID 20151545—

反応手順

2.9 ml of a solution of 5.9N hydrogen chloride in ethanol were added to a solution of 5 g of the product of Example 1 in 5 ml of ethanol and the mixture was stirred while adding isopropyl ether thereto. The mixture was stirred for 24 hours and was filtered. The product was empasted with isopropyl ether, filtered and dried under pressure to obtain 4.4 g of 3,4-bis-(4-methoxyphenyl)-5-ethyl-4H-1,2,4-triazole hydrochloride.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04659729
出典データセットuspto-grants-1987_04
ORD IDord-443474a511404915bd3fcb8dc9d678f8
出典メモuspto-grants-1987_04