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2',4'-Dihydroxyacetophenone → Ethyl hexanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2',4'-Dihydroxyacetophenone | HCID 6990 | — |
| 反応物 | Ethyl 6-(4-benzylphenyl)-6-bromo-hexanoate | HCID 13881964 | — |
| 生成物 | Ethyl hexanoate | HCID 31265 | — |
反応手順
Following the procedure of Example 15, 3.75 g. of ethyl 6-(4-benzylphenyl)-6-bromo-hexanoate and 1.94 g. of 2,4-dihydroxyacetophenone were reacted to provide the intermediate ethyl hexanoate derivative which was then hydrolyzed to provide 0.95 g. of the title product as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04661505 |
| 出典データセット | uspto-grants-1987_04 |
| ORD ID | ord-75e0d54fe36542b586511d33af2d95ca |
| 出典メモ | uspto-grants-1987_04 |