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n-Butyl-2,2,6,6-tetramethyl-4-piperidinamine → 1,3-bis[2-(N-butyl-N-(2,2,6,6-tetramethyl-4-piperidyl)amino)5-ethyl-1,3,2-dioxaphosphorinan-5-yl]-2-oxapropane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | n-Butyl-2,2,6,6-tetramethyl-4-piperidinamine | HCID 118285 | — |
| 反応物 | 1,3-Bis(2-chloro-5-ethyl-1,3,2-dioxaphosphorinan-5-yl)-2-oxapropane | HCID 21277950 | — |
| 生成物 | 1,3-bis[2-(N-butyl-N-(2,2,6,6-tetramethyl-4-piperidyl)amino)5-ethyl-1,3,2-dioxaphosphorinan-5-yl]-2-oxapropane | HCID 21277935 | — |
反応手順
If 1,3-bis(2-chloro-5-ethyl-1,3,2-dioxaphosphorinan-5-yl)-2-oxapropane is reacted with 4-butylamino-2,2,6,6-tetramethylpiperidine in a procedure analogous to Example 2, 1,3-bis[2-(N-butyl-N-(2,2,6,6-tetramethyl-4-piperidyl)amino)-5-ethyl-1,3,2-dioxaphosphorinan-5-yl]-2-oxapropane is obtained as a viscous resin (Compound No. 22, formula below, R3 =H); FD-MS: 730 (M+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04661594 |
| 出典データセット | uspto-grants-1987_04 |
| ORD ID | ord-719cfde8987d4b929abe35dc82f81a9d |
| 出典メモ | uspto-grants-1987_04 |