2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate

HRID 543455

反応式

HRID 543455 の反応式
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]

参加物

4

反応物 2

HCID 331012-Propenoic acid, 3-hydroxypropyl esterHCID 557541Isopropenylphosphonic acid

生成物 1

HCID 86739384Isopropenylphosphonic Acid Hydroxypropylacrylate

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.

後処理

  1. customThe bulk of the polymer crystallized during the first period
  2. temperatureof reflux

出典と根拠

ORDレコード
ord-49e0e65a7ace49c29f56fbb104f02e73
出典データセット
uspto-grants-1984_05
特許番号
US04446028

関連ノート

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