2-Propenoic acid, 3-hydroxypropyl ester → Isopropenylphosphonic Acid Hydroxypropylacrylate
反応式
[C:1]([P:4](=[O:7])([OH:6])[OH:5])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]>O>[C:1]([P:4](=[O:5])([OH:7])[OH:6])([CH3:3])=[CH2:2].[OH:8][CH2:9][CH2:10][CH2:11][O:12][C:13](=[O:16])[CH:14]=[CH2:15]参加物
4
実験手順
Used the method of Example 5, isopropenyl phosphonic acid (30.7 g, 54%, 0.14 mole), hydroxypropylacrylate (36.4 g, 0.28 mole) and water (144.9 g) were charged in the reactor. The bulk of the polymer crystallized during the first period of reflux and was found to be insoluble in water.
後処理
- customThe bulk of the polymer crystallized during the first period
- temperatureof reflux
出典と根拠
- ORDレコード
- ord-49e0e65a7ace49c29f56fbb104f02e73
- 出典データセット
- uspto-grants-1984_05
- 特許番号
- US04446028
反応ノート
読み込み中…