Hydrochloric Acid → HCID 178458047、化合物
反応式
C([NH:4][CH2:5][CH:6]([N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)[CH3:7])(=O)C.[ClH:14]>>[ClH:14].[NH2:4][CH2:5][CH:6]([N:8]1[C:12]([SH:13])=[N:11][N:10]=[N:9]1)[CH3:7]参加物
3
実験手順
A mixture of 1-[1-(acetamidomethyl)ethyl]-1H-tetrazole-5-thiol (23 g) and 6 N aqueous hydrochloric acid (300 ml) was refluxed for 2 hours under stirring and evaporated to dryness. The residue was triturated with diethyl ether to give 1-[1-(aminomethyl)ethyl]-1H-tetrazole-5-thiol hydrochloride (19 g), mp 208° to 210° C.
後処理
- temperaturewas refluxed for 2 hours
- customevaporated to dryness
- customThe residue was triturated with diethyl ether
出典と根拠
- ORDレコード
- ord-77ea3384e3b94a37bbccab2e8e9d5580
- 出典データセット
- uspto-grants-1984_05
- 特許番号
- US04447429
反応ノート
読み込み中…