Hydrochloric Acid → HCID 131713514、化合物

HRID 544545

反応式

HRID 544545 の反応式
[Cl-].[Na+].[CH3:3][P:4]([CH2:6][CH2:7][P:8]([CH3:10])[CH3:9])[CH3:5].Cl.[CH2:12]([OH:14])[CH3:13]>>[CH2:12]([OH:14])[CH3:13].[CH3:3][P:4]([CH2:6][CH2:7][P:8]([CH3:10])[CH3:9])[CH3:5]

参加物

5

反応物 4

HCID 313Hydrochloric AcidHCID 702Ethanol2 回HCID 5234Sodium Chloride2 回HCID 1410591,2-Bis(dimethylphosphino)ethane

生成物 1

HCID 131713514HCID 131713514、化合物収率 80%

実験手順

Prepare a saturated solution of sodium chloride in ethanol by dissolving 117 mg of sodium chloride in 20 ml of degassed ethanol. Add 11.1 μl of liquid DMPE to this solution and adjust its pH to approximately 2.25 by adding concentrated hydrochloric acid. Dispense 5 ml into a 10 cc vial and crimp seal it using a teflon-coated stopper. Inject approximately 5 mCi of 99mTc-pertechnetate eluate into the vial and place it in a boiling water bath for 1 hour. HPLC analysis shows a yield of greater than 80% of the [99mTcCl2 (DMPE)2 ]+ complex.

後処理

  1. customDispense 5 ml into a 10 cc vial and crimp seal it

出典と根拠

ORDレコード
ord-9a0dc57b1aae4ff8b16c6303cf18cc6d
出典データセット
uspto-grants-1984_05
特許番号
US04451450

関連ノート

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