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Dimethyl Sulfoxide → HCID 67171755、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyl Sulfoxide | HCID 679 | — |
| 反応物 | p-Fluoronitrobenzene | HCID 9590 | — |
| 反応物 | 1-(2-Ethoxyethyl)piperazine | HCID 2734643 | — |
| 生成物 | HCID 67171755 | HCID 67171755 | — |
反応手順
In the same manner as in Production Example 5-1, but using 4-(2-ethoxyethyl)piperazine in place of N-ethylpiperazine used in Production Example 5-1, using 4-nitrofluorobenzene in place of 2-fluoro-5-nitrobenzyl alcohol, and using dimethylsulfoxide in place of N-methylpyrrolidone, 1.50 g of the entitled compound was obtained as a yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07935708B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-065667ded40b4a6ab17689ef360b5e8c |
| 出典メモ | uspto-grants-2011_05 |