化工社化工社 化学情報印刷レポート · 研究参考用
Benzene, 1-fluoro-2-methyl-4-nitro- → HCID 61151226、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene, 1-fluoro-2-methyl-4-nitro- | HCID 68001 | — |
| 反応物 | Diisopropylethylamine | HCID 81531 | — |
| 反応物 | 1-(2-Ethoxyethyl)piperazine | HCID 2734643 | — |
| 溶媒 | Dimethyl Sulfoxide | HCID 679 | — |
| 生成物 | HCID 61151226 | HCID 61151226 | — |
反応手順
In the same manner as in Production Example 5-1, but using 4-(2-ethoxyethyl)piperazine in place of N-ethylpiperazine used in Production Example 5-1, using 5-nitro-2-fluorotoluene in place of 2-fluoro-5-nitrobenzyl alcohol, using N,N-diisopropylethylamine in place of potassium carbonate, and using dimethylsulfoxide in place of N-methylpyrrolidone, the entitled compound was obtained as a yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07935708B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-1118415f06c340358225aa91bac29e97 |
| 出典メモ | uspto-grants-2011_05 |