反応式
C1(CCN2C3C(=CC=CC=3)C(=O)C2=O)CC1.[C:17]1([CH:23]([C:35]2[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26](=[O:33])[C:25]2=[O:34])[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1.O1C2C=CC(O)=CC=2OC1.[F:51][C:52]([F:62])([F:61])[O:53][C:54]1[CH:55]=[C:56]([OH:60])[CH:57]=[CH:58][CH:59]=1>>[C:35]1([CH:23]([C:17]2[CH:18]=[CH:19][CH:20]=[CH:21][CH:22]=2)[N:24]2[C:32]3[C:27](=[CH:28][CH:29]=[CH:30][CH:31]=3)[C:26]([OH:33])([C:57]3[CH:58]=[CH:59][C:54]([O:53][C:52]([F:61])([F:62])[F:51])=[CH:55][C:56]=3[OH:60])[C:25]2=[O:34])[CH:40]=[CH:39][CH:38]=[CH:37][CH:36]=1参加物
5
実験手順
Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-(diphenylmethyl)-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 3-(trifluoromethoxy)phenol, the title compound was obtained (75%): MS (ES+) m/z 514.5 (M+23).
出典と根拠
- ORDレコード
- ord-1da43332e4df42dcb5dcbf7daf64883f
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- US07935721B2
関連ノート
読み込み中…