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Succinyl chloride → Phenylboronic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Succinyl chloride | HCID 10970 | — |
| 反応物 | Adipoyl chloride | HCID 61034 | — |
| 反応物 | Carbonic acid, bis(2-methylpropyl) ester | HCID 68321 | — |
| 反応物 | 3-Aminophenylboronic acid | HCID 92269 | — |
| 反応物 | 2,2'-[Oxybis(ethyleneoxy)]bisacetyl dichloride | HCID 11276940 | — |
| 反応物 | 3,6,9-Trioxaundecanedioic acid diisobutylcarbonate | HCID 86750731 | — |
| 生成物 | Phenylboronic Acid | HCID 66827 | — |
反応手順
Phenylboronic acid reagents of General Formula IX are prepared by condensation of (3-aminophenyl)boronic acid with an activated dicarboxylic acid preferably selected from, but not limited to, either succinyl chloride, adipoyl chloride, adiptic acid diisobutylcarbonate, suberoyl chloride,3,3'-dithiopropionyl chloride and 3,6,9-trioxaundecanedioyl chloride and 3,6,9-trioxaundecanedioic acid diisobutylcarbonate. The preparation of a single reagent of General Formula IX has been previously reported (Burnett, T. J., Peebles, H. C. and Hageman, J. H. (1980) Biochem. Biophys. Research Commun., 96, 157-162). ##STR11##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05623055 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-01a857b0647247a5ae68bd41c6dace10 |
| 出典メモ | uspto-grants-1997_04 |