tert-butyl N'-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate → 5-Chloro-2-cyclohexyl-valeric acid hydrazide hydrochloride
反応式
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1)[C:6]([NH:8][NH:9]C(OC(C)(C)C)=O)=[O:7]>Cl.O1CCOCC1>[ClH:1].[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([CH:17]1[CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1)[C:6]([NH:8][NH2:9])=[O:7]参加物
4
実験手順
tert-Butyl N′-(5-chloro-2-cyclohexyl-pentanoyl)-hydrazinecarboxylate (155 mg) was dissolved in a solution of 4 N hydrogen chloride in dioxane (2 ml), and the reaction solution was stirred at room temperature for one hour. The reaction solution was concentrated under reduced pressure to obtain 144 mg of the title compound. The property value of the compound is as follows.
後処理
- concentrationThe reaction solution was concentrated under reduced pressure
出典と根拠
- ORDレコード
- ord-3003b35eed6748cfa68010ac9fd15804
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- US07935815B2
反応ノート
読み込み中…