化工社化工社 化学情報印刷レポート · 研究参考用
TIBA isododecane → 2,3,5-Triiodobenzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | TIBA isododecane | HCID 131728349 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2,3,5-Triiodobenzoic acid | HCID 6948 | — |
反応手順
33.3 ml of TIBA/isododecane solution (101 g/L) was mixed with 7.9 cc of MAO/toluene solution (Albemarle −30% wt) to obtain a MAO/TIBA molar ratio of 2:1. The solution was stirred for 1 hour at room temperature. Then, 69 mg of A-1 was dissolved in the solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07943716B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-7c8ef107c3634e86a66b5e20aa7b8cba |
| 出典メモ | uspto-grants-2011_05 |