化工社化工社 化学情報印刷レポート · 研究参考用
5-Phenylthiophene-2-carbaldehyde → 3-Bromo-2-fluoro-6-methyl-1-(5-phenyl-2-thienylmethyl)benzene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Phenylthiophene-2-carbaldehyde | HCID 177053 | — |
| 反応物 | 4-Bromo-3-fluorotoluene | HCID 573280 | — |
| 生成物 | 3-Bromo-2-fluoro-6-methyl-1-(5-phenyl-2-thienylmethyl)benzene | HCID 66608527 | — |
反応手順
4-Bromo-3-fluorotoluene and 5-phenyl-2-thiophenecarboxaldehyde were treated in a manner similar to Reference Example 116 to give the target compound as pale blue powders. APCI-Mass m/Z 361/363 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07943788B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-59809dccd2824e33bf09d80dec4dcc27 |
| 出典メモ | uspto-grants-2011_05 |