2,4-Dimethylthiazole-5-carbohydrazide → 4-methyl-3-(4-methyl-1,3-thiazol-5-yl)-5-(4-penten-1-yl)-4H-1,2,4-triazole
反応式
C[C:2]1[S:3][C:4]([C:8]([NH:10][NH2:11])=O)=[C:5]([CH3:7])[N:6]=1.Cl.[CH3:13][NH:14][C:15](=NC)[CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20]>>[CH3:13][N:14]1[C:15]([CH2:16][CH2:17][CH2:18][CH:19]=[CH2:20])=[N:11][N:10]=[C:8]1[C:4]1[S:3][CH:2]=[N:6][C:5]=1[CH3:7]参加物
3
実験手順
The title compound was prepared in analogy to Preparation 11 in 0.31 g yield starting from 2,4-dimethyl-thiazole-5-carboxylic acid hydrazide (0.52 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.58 g). MS (m/z): 249 [MH]+.
後処理
- customyield
出典と根拠
- ORDレコード
- ord-a69be5f9d8f2491fb78534d8907da9cf
- 出典データセット
- uspto-grants-2011_05
- 特許番号
- US07947683B2
反応ノート
読み込み中…