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4-Methoxybenzohydrazide → 4-methyl-3-[4-(methyloxy)phenyl]-5-(4-penten-1-yl)-4H-1,2,4-triazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxybenzohydrazide | HCID 76792 | — |
| 反応物 | N,N'-dimethyl-5-hexenimidamide hydrochloride | HCID 86630240 | — |
| 生成物 | 4-methyl-3-[4-(methyloxy)phenyl]-5-(4-penten-1-yl)-4H-1,2,4-triazole | HCID 57691938 | — |
反応手順
The title compound was prepared in analogy to Preparation 11 in 0.12 g yield starting from 4-methoxybenzhydrazide (0.5 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.48 g). MS (m/z): 258 [MH]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07947683B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-dd747487230141da887e8c7b4864273f |
| 出典メモ | uspto-grants-2011_05 |