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2-Fluorobenzhydrazide → 3-(2-fluorophenyl)-4-methyl-5-(4-penten-1-yl)-4H-1,2,4-triazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Fluorobenzhydrazide | HCID 136288 | — |
| 反応物 | N,N'-dimethyl-5-hexenimidamide hydrochloride | HCID 86630240 | — |
| 生成物 | 3-(2-fluorophenyl)-4-methyl-5-(4-penten-1-yl)-4H-1,2,4-triazole | HCID 57691867 | — |
反応手順
The title compound was prepared in analogy to Preparation 11 in 0.23 g yield starting from 2-fluorobenzoic hydrazide (0.44 g) and N,N′-dimethyl-5-hexenimidamide hydrochloride (0.50 g). MS (m/z): 245 [MH]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07947683B2 |
| 出典データセット | uspto-grants-2011_05 |
| ORD ID | ord-2ab0778f35204d109aacface2ab2b848 |
| 出典メモ | uspto-grants-2011_05 |