Acetic Anhydride → N-[2-(4,5-Dimethyl-thiophen-2-yl)-ethyl]-acetamide

反応式

[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][NH2:10])[S:5][C:6]=1[CH3:7].[C:11](OC(=O)C)(=[O:13])[CH3:12]>>[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][NH:10][C:11](=[O:13])[CH3:12])[S:5][C:6]=1[CH3:7]

参加物

反応物 2

HCID 7918Acetic Anhydride

HCID 530135252-(4,5-Dimethyl-thiophen-2-yl)-ethylamine

生成物 1

HCID 59663060N-[2-(4,5-Dimethyl-thiophen-2-yl)-ethyl]-acetamide収率 79%

実験手順

In close analogy to the procedure described above, 2-(4,5-Dimethyl-thiophen-2-yl)-ethylamine is reacted with acetic anhydride to provide the title compound.

出典と根拠

ORDレコード: ord-9b73af21af4140ac8769ff493a85cb48
出典データセット: uspto-grants-2011_05
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07947689B2

反応ノート

読み込み中…