反応式
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][C:9]2[C:18]3[C:13](=[CH:14][C:15]([C:19]([F:22])([F:21])[F:20])=[CH:16][CH:17]=3)[N:12]=[CH:11][CH:10]=2)=[CH:4][CH:3]=1.[Cl:23][C:24]1[CH:29]=[CH:28][C:27]([N:30]=[C:31]=[S:32])=[CH:26][C:25]=1[C:33]([F:36])([F:35])[F:34]>>[F:20][C:19]([F:22])([F:21])[C:15]1[CH:14]=[C:13]2[C:18]([C:9]([S:8][C:5]3[CH:6]=[CH:7][C:2]([NH:1][C:31]([NH:30][C:27]4[CH:28]=[CH:29][C:24]([Cl:23])=[C:25]([C:33]([F:36])([F:34])[F:35])[CH:26]=4)=[S:32])=[CH:3][CH:4]=3)=[CH:10][CH:11]=[N:12]2)=[CH:17][CH:16]=1参加物
3
実験手順
4-(4-aminophenylthio)-7-trifluoromethylquinoline (0.01 mole, 3.2 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate (0.01 mole, 2.4 g) were reacted according to procedure C to yield the title compound 3.5 g, 63%. Mass Spec (FD) 557. Calculated for C24H14ClF6N3S2 : C, 51.66; H, 2.53; N, 7.53. Found: C, 51.92; H, 2.53; N, 7.46.
出典と根拠
- ORDレコード
- ord-01b516bc3ddb49af813ed34ded8f4123
- 出典データセット
- uspto-grants-1997_04
- 特許番号
- US05624937
関連ノート
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