化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → o-Tolyl-acetyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | o-Tolylacetic acid | HCID 69519 | — |
| 生成物 | o-Tolyl-acetyl chloride | HCID 2760632 | — |
反応手順
A solution of 2.0 g of o-tolylacetic acid in 27 ml of thionyl chloride is heated at reflux for 1 hour. The volatiles are evaporated in vacuo to give a residue which is concentrated from toluene three times and dried under vacuum to give 2.1 g of the desired product as a light brown oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05624923 |
| 出典データセット | uspto-grants-1997_04 |
| ORD ID | ord-9e3ada643d264e1abb01d8e9bf8ac9c6 |
| 出典メモ | uspto-grants-1997_04 |