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HRID 554497作成日:2026年10月25日

HCID 12660316、化合物 → 2-Benzylphenol

https://huagongshe.com/reaction/554497

反応式

関与物質

役割名称HCID仕込み量
反応物HCID 12660316HCID 12660316—
触媒Palladium hydroxideHCID 9942167—
溶媒MethanolHCID 887—
生成物2-BenzylphenolHCID 2421667%

反応手順

To a solution of 2-(4-chlorobenzyl)phenol (618.5 mg, 2.83 mmol) in methanol (20 mL), a 20% palladium hydroxide catalyst (240 mg) was added. The mixture was stirred under a hydrogen atmosphere for three days, and then the catalyst was filtered off. The solvent was distilled under reduced pressure and the obtained residue was purified by silica gel column chromatography [developing solution=ethyl acetate:n-hexane (1:4)] to obtain the title compound (348.4 mg, 67%).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08048897B2
出典データセットuspto-grants-2011_11
ORD IDord-882e0f4fdfcf4a8086b0b4f0864124f9
出典メモuspto-grants-2011_11