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HRID 556119作成日:2026年10月27日

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester → Hydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester

https://huagongshe.com/reaction/556119

反応式

関与物質

役割名称HCID仕込み量
反応物Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667396—
触媒PalladiumHCID 23938—
溶媒MethanolHCID 887—
生成物Hydroxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl esterHCID 57667367—

反応手順

Benzyloxy-acetic acid 5-chloro-2-(2,4-dichloro-phenoxy)-phenyl ester 4 (5 grams) was dissolved in methanol (50 mL) in a pressure vessel, palladium on carbon (5%, 5 grams) was added and the mixture was stirred under an atmosphere of hydrogen (4 Kg) for 4 hours. The catalyst was removed by filtration and the methanol was distilled off to yield crude 5.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08053591B2
出典データセットuspto-grants-2011_11
ORD IDord-0f12a1e9abed4036bae5e61234a369c1
出典メモuspto-grants-2011_11