化工社化工社 化学情報印刷レポート · 研究参考用
N,N-Dimethyl-N-decylamine → N-(4-vinylbenzyl)-N-decyl-N,N-dimethylammonium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N,N-Dimethyl-N-decylamine | HCID 70711 | — |
| 反応物 | p-Vinylbenzyl chloride | HCID 74126 | — |
| 生成物 | N-(4-vinylbenzyl)-N-decyl-N,N-dimethylammonium chloride | HCID 86612068 | — |
反応手順
4-Vinylbenzyl chloride (18.60 g, 100 mmol) and N,N-dimethyl-N-decylamine (15.26 g, 100 mmol) were mixed in a 100 mL round bottomed flask. The mixture was allowed to sit overnight. The crystalline product was crushed and washed with ether. The product was collected by filtration (30.3 g, 90%)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08058208B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-d39455f6861e4af48fbccb83a3fd311d |
| 出典メモ | uspto-grants-2011_11 |