反応式
[CH2:1]([C:8]#[N:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:10][OH:11].ON=C(N)C1C=CC=CC=1>CCO>[OH:11][N:10]=[C:8]([NH2:9])[CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1参加物
5
実験手順
Benzyl cyanide (1 g, 8.5 mmol) and hydroxylamine (50% in water, 1.04 cm3, 17 mmol, 2 eq) in EtOH (8.5 cm3) were reacted in the same manner as in the preparation of N′-hydroxybenzimidamide (EtOAc used in extraction) to give the product N′-hydroxy-2-phenylacetimidamide (1.04 g, 81.9%) as a pale yellow solid, mp 63.5-64.5° C. (lit 57-59° C.).
出典と根拠
- ORDレコード
- ord-7126ea936ddf4af08606b069eb5d41bb
- 出典データセット
- uspto-grants-2011_11
- 特許番号
- US08062429B2
関連ノート
読み込み中…