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Acetic Acid → N'-(4-Iodophenyl)acetohydrazide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | 4-Iodophenylhydrazine | HCID 704591 | — |
| 生成物 | N'-(4-Iodophenyl)acetohydrazide | HCID 623860 | — |
反応手順
A mixture of 10 g of 4-iodophenylhydrazine in 80 ml of acetic acid is refluxed for 5 hours. The reaction mixture is concentrated under vacuum, the residue is taken up with water, and the precipitate formed is filter-dried and washed with a propan-2-ol/PE (50/50; v/v) mixture. 9 g of the expected compound are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08063061B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-bc6017e9c2914504b8961b1c59b6217f |
| 出典メモ | uspto-grants-2011_11 |