化工社化工社 化学情報印刷レポート · 研究参考用
4-Fluorobenzaldehyde → (4-Chloro-2-methylphenyl)(4-fluorophenyl)methanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Fluorobenzaldehyde | HCID 68023 | — |
| 反応物 | 2-Bromo-5-chlorotoluene | HCID 84476 | — |
| 反応物 | alpha-(4-Fluorophenyl)-4-(trifluoromethyl)benzenemethanol | HCID 579773 | — |
| 生成物 | (4-Chloro-2-methylphenyl)(4-fluorophenyl)methanol | HCID 58392095 | — |
反応手順
The title compound was prepared starting from 1.00 g (4.87 mmol) of 2-bromo-5-chlorotoluene and 0.72 g (5.84 mmol) of 4-fluorobenzaldehyde in analogy to the synthesis of the compound from Example 80A. 0.64 g (52% of theory) of the title compound was obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08063234B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-bef130b1c5ae4c6dac3ab49c24c06c69 |
| 出典メモ | uspto-grants-2011_11 |