戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 561893作成日:2026年10月27日

Ethyl cyanoacetate → Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-

https://huagongshe.com/reaction/561893

反応式

関与物質

役割名称HCID仕込み量
反応物Ethyl cyanoacetateHCID 7764—
反応物HexaneHCID 8058—
反応物Benzaldehyde, 4-(2-hydroxyethoxy)-HCID 89178—
溶媒EthanolHCID 702—
生成物Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-HCID 50742116—

反応手順

Ethyl cyanoacetate (1.1 eq.) and 4-(2-hydroxyethoxy)benzaldehyde (1 eq.) were combined in ethanol (1.2 M). The reaction mixture was stirred at RT for 48. To this was then added an equal volume of hexane and the title compound was isolated by filtration as a pale yellow solid.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US08063105B2
出典データセットuspto-grants-2011_11
ORD IDord-1040e73697ea45ebbefdd1e7f8935a97
出典メモuspto-grants-2011_11