化工社化工社 化学情報印刷レポート · 研究参考用
Ethyl cyanoacetate → Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethyl cyanoacetate | HCID 7764 | — |
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | Benzaldehyde, 4-(2-hydroxyethoxy)- | HCID 89178 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Poly(oxy-1,2-ethanediyl), alpha-[4-(2-cyano-3-ethoxy-3-oxo-1-propenyl)phenyl]-omega-hydroxy- | HCID 50742116 | — |
反応手順
Ethyl cyanoacetate (1.1 eq.) and 4-(2-hydroxyethoxy)benzaldehyde (1 eq.) were combined in ethanol (1.2 M). The reaction mixture was stirred at RT for 48. To this was then added an equal volume of hexane and the title compound was isolated by filtration as a pale yellow solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08063105B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-1040e73697ea45ebbefdd1e7f8935a97 |
| 出典メモ | uspto-grants-2011_11 |