化工社化工社 化学情報印刷レポート · 研究参考用
Sulfur dichloride → 3-(3-Fluorophenyl)propanoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfur dichloride | HCID 25353 | — |
| 反応物 | 3-(3-Fluorophenyl)propionic acid | HCID 2737489 | — |
| 生成物 | 3-(3-Fluorophenyl)propanoyl chloride | HCID 18993501 | — |
反応手順
A mixture of 3-(3-fluorophenyl)propanoic acid (2.50 g, 14.9 mmol) and dichlorosulfane (10 mL) under N2 was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound, which was used for next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09434695B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-119617a6c7804e7aa0f70ecb08b9ebb9 |
| 出典メモ | uspto-grants-2016_09 |