化工社化工社 化学情報印刷レポート · 研究参考用
Sulfur dichloride → 4-(3-Fluorophenoxy)butanoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfur dichloride | HCID 25353 | — |
| 反応物 | 4-(3-Fluorophenoxy)butanoic acid | HCID 6486015 | — |
| 生成物 | 4-(3-Fluorophenoxy)butanoyl chloride | HCID 90023167 | — |
反応手順
A solution of 4-(3-fluorophenoxy)butanoic acid (3.00 g, 15.1 mmol) in dichlorosulfane (15 mL) under N2 was refluxed for 3 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound, which was used for next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09434695B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-f4e72ac7cd384758b6534f103e26e766 |
| 出典メモ | uspto-grants-2016_09 |