化工社化工社 化学情報印刷レポート · 研究参考用
Sulfur dichloride → 2-(Cyclohexyloxy)acetyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sulfur dichloride | HCID 25353 | — |
| 反応物 | Cyclohexoxyacetic acid | HCID 191994 | — |
| 生成物 | 2-(Cyclohexyloxy)acetyl chloride | HCID 12484123 | — |
反応手順
A mixture of 2-(cyclohexyloxy)acetic acid (0.90 g, 5.69 mmol) and dichlorosulfane (10 mL) was refluxed for 2 h. The mixture was cooled to rt and concentrated in vacuo to give the title compound as yellow oil, which was used for next step without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09434695B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-8af8cc706d3a457badbaab90d0f5f777 |
| 出典メモ | uspto-grants-2016_09 |