化工社化工社 化学情報印刷レポート · 研究参考用
Thiophosgene → HCID 178424321、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thiophosgene | HCID 10040 | — |
| 反応物 | N-(4-Amino-o-tolyl)-4-chlorophthalimide | HCID 93991 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | HCID 178424321 | HCID 178424321 | 148.1% |
反応手順
To a slurry of 150 mg (0.52 mmol) of 2-(4-amino-2-methylphenyl)-5-chlorobenzo[c]azoline-1,3-dione in 2 mL of acetone, was added 41 uL (0.54 mmol) of thiophosgene. The yellow slurry dissolved whereupon a white precipitate formed. After 1 h, this solid was collected by filtration and dried to give 127 mg (74%) of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08067428B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-78146cea97d8469c867aee23ad5403e4 |
| 出典メモ | uspto-grants-2011_11 |