化工社化工社 化学情報印刷レポート · 研究参考用
a Farnesol → 3,7,11-Trimethyl-1-dodecanol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | a Farnesol | HCID 3327 | — |
| 触媒 | Platinum oxide (PtO) | HCID 82844 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 3,7,11-Trimethyl-1-dodecanol | HCID 138824 | 94.9% |
反応手順
Farnesol (200 g) was dissolved in ethanol (1000 ml), added with platinum oxide (1 g) and stirred for 24 hours at room temperature under hydrogen atmosphere. After the completion of the reaction, insoluble material was removed by filtration through a Celite layer and the filtrate was concentrated under reduced pressure to obtain 3,7,11-trimethyldodecanol (195 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05245070 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-d6aa1484224448e995eff7bbe4db6fd5 |
| 出典メモ | uspto-grants-1993_09 |