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Dimethyldioxirane → 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyldioxirane | HCID 115197 | — |
| 反応物 | 8-Benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one | HCID 22499178 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 8-Benzyloxy-3-methyl5-oxiranyl-1H-quinolin-2-one | HCID 57494231 | — |
反応手順
To 8-benzyloxy-3-methyl-5-vinyl-1H-quinolin-2-one (300 mg) is added to a 0.1M solution of dimethyldioxirane in acetone (12.4 mL). After stirring at room temperature for 2 hours, the solvent is removed in vacuo to yield the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08067437B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-3b06ed7260654a95b9d202fd1a4993f3 |
| 出典メモ | uspto-grants-2011_11 |