化工社化工社 化学情報印刷レポート · 研究参考用
Pentamethylbenzene → Methyl 2-(3-cyano-4-hydroxyphenyl)isonicotinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pentamethylbenzene | HCID 12784 | — |
| 反応物 | Methyl 2-[4-(benzyloxy)-3-cyanophenyl]isonicotinate | HCID 66995135 | — |
| 溶媒 | Trifluoroacetic acid | HCID 6422 | — |
| 生成物 | Methyl 2-(3-cyano-4-hydroxyphenyl)isonicotinate | HCID 136368377 | — |
反応手順
Methyl 2-[4(benzyloxy)-3-cyanophenyl]isonicotinate and pentamethylbenzene were heated under reflux temperature in trifluoroacetic acid to obtain methyl 2-(3-cyano-4-hydroxyphenyl)isonicotinate. F: 255.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08067446B2 |
| 出典データセット | uspto-grants-2011_11 |
| ORD ID | ord-b435b5fd0d6c49fc90b0c27c34855dbd |
| 出典メモ | uspto-grants-2011_11 |