Ethanol → Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate

HRID 563531

反応式

HRID 563531 の反応式
[Br:1][C:2]1[CH:3]=[C:4]([CH2:9][C:10]([OH:12])=[O:11])[CH:5]=[CH:6][C:7]=1[OH:8].S(=O)(=O)(O)O.[CH3:18][CH2:19]O>>[CH2:18]([O:11][C:10](=[O:12])[CH2:9][C:4]1[CH:5]=[CH:6][C:7]([OH:8])=[C:2]([Br:1])[CH:3]=1)[CH3:19]

参加物

4

反応物 3

HCID 702EthanolHCID 1118Sulfuric AcidHCID 27696283-Bromo-4-hydroxyphenylacetic acid

生成物 1

HCID 18620106Ethyl 2-(3-bromo-4-hydroxyphenyl)acetate

実験手順

(3-Bromo-4-hydroxy-phenyl)-acetic acid (5.6 mmol) in EtOH (20 mL) was treated with sulfuric acid (1 mL) and stirred at room temperature over the weekend. The mixture was concentrated to give the title compound.

後処理

  1. concentrationThe mixture was concentrated

出典と根拠

ORDレコード
ord-434516121a0b4996ae885f5f0b5347c6
出典データセット
uspto-grants-2011_11
特許番号
US08067445B2

関連ノート

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