Ethylamine → (2'-Ethylaminomethyl-6-methoxy-5'-methyl-biphenyl-3-yl)-acetic acid ethyl ester

HRID 563739

反応式

HRID 563739 の反応式
[CH2:1]([O:3][C:4](=[O:23])[CH2:5][C:6]1[CH:7]=[C:8]([C:14]2[CH:19]=[C:18]([CH3:20])[CH:17]=[CH:16][C:15]=2[CH:21]=O)[C:9]([O:12][CH3:13])=[CH:10][CH:11]=1)[CH3:2].[CH2:24]([NH2:26])[CH3:25]>>[CH2:1]([O:3][C:4](=[O:23])[CH2:5][C:6]1[CH:7]=[C:8]([C:14]2[CH:19]=[C:18]([CH3:20])[CH:17]=[CH:16][C:15]=2[CH2:21][NH:26][CH2:24][CH3:25])[C:9]([O:12][CH3:13])=[CH:10][CH:11]=1)[CH3:2]

参加物

3

反応物 2

HCID 6341EthylamineHCID 58148809(2'-Formyl-6-methoxy-5'-methyl-biphenyl-3-yl)-acetic acid ethyl ester

生成物 1

HCID 58149093(2'-Ethylaminomethyl-6-methoxy-5'-methyl-biphenyl-3-yl)-acetic acid ethyl ester

実験手順

Prepared according to the procedure described in Example 33, Step 4, using the following starting materials: (2′-formyl-6-methoxy-5′-methyl-biphenyl-3-yl)-acetic acid ethyl ester and ethylamine (2M in THF).

後処理

  1. customPrepared

出典と根拠

ORDレコード
ord-7cf1d9474ad44fbfa08285ecf8f2f834
出典データセット
uspto-grants-2011_11
特許番号
US08067445B2

関連ノート

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