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Bisphenol A → Phenol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bisphenol A | HCID 6623 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Phenol | HCID 996 | — |
| 生成物 | Bisphenol A | HCID 6623 | — |
反応手順
The process of preparing high purity bisphenol A by crystallizing the adduct of bisphenol A with phenol (hereinafter referred to as bisphenol A-phenol adduct) has been disclosed, for example, in Japanese Patent Publication SHO 63-26735(1988). That is, a phenol solution of bisphenol A which was prepared in the presence of a hydrochloric acid catalyst is cooled to a range of 35° to 70° C. while feeding 2 to 20% by weight of water to the solution under reduced pressure, precipitated crystals of bisphenol A-phenol adduct are filtered to separate the crystals, and phenol is evaporated from the crystals to obtain high purity bisphenol A.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05245088 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-38c85ad4634b442cbe5132fd78f0ba93 |
| 出典メモ | uspto-grants-1993_09 |