関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Azobisisobutyronitrile | HCID 6547 | — |
| 反応物 | tert-Butyl methacrylate | HCID 11448 | — |
| 反応物 | 2-Naphthyl methacrylate | HCID 82654 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | tert-Butyl methacrylate | HCID 11448 | — |
| 生成物 | Naphthyl methacrylate | HCID 4064248 | — |
反応手順
0.3 mol of 2-naphthyl methacrylate and 0.7 mol of tert-butyl methacrylate were mixed with 200 g of toluene, and 2 g of azoisobutylonitrile (AIBN) was added thereto. The mixed system was heated at a temperature of 70° C. for 8 hours and then purified by dropping it into acetone-methanol solvent, to obtain a copolymer of naphthyl methacrylate and tert-butyl methacrylate (Resin A).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06168897A |
|---|
| 出典データセット | uspto-grants-2001_01 |
|---|
| ORD ID | ord-619dddc516084022b85e8f2c0b3b2efb |
|---|
| 出典メモ | uspto-grants-2001_01 |
|---|
