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HRID 565077作成日:2026年10月26日

Phthalic Anhydride → 2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acid

https://huagongshe.com/reaction/565077

反応式

関与物質

役割名称HCID仕込み量
反応物Phthalic AnhydrideHCID 6811—
反応物3-(Diethylamino)phenolHCID 7062—
溶媒TolueneHCID 1140—
生成物2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acidHCID 79878—

反応手順

2-(2′-Carboxybenzoyl)-5-diethylaminophenol was prepared as follows. A mixture of m-diethylaminophenol (1 mole) and phthalic anhydride (1.2 moles) was refluxed in toluene (2.0 L) for about 16 hours, cooled, and the resulting solid filtered, washed with toluene and dried to give 2-(2′-carboxybenzoyl)-5-diethylaminophenol in 70% yield.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06169185A
出典データセットuspto-grants-2001_01
ORD IDord-6101d14e85e44ff5aac0ecc59b3cd271
出典メモuspto-grants-2001_01