化工社化工社 化学情報印刷レポート · 研究参考用
Phthalic Anhydride → 2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | 3-(Diethylamino)phenol | HCID 7062 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | 2-[4-(Diethylamino)-2-hydroxybenzoyl]benzoic acid | HCID 79878 | — |
反応手順
2-(2′-Carboxybenzoyl)-5-diethylaminophenol was prepared as follows. A mixture of m-diethylaminophenol (1 mole) and phthalic anhydride (1.2 moles) was refluxed in toluene (2.0 L) for about 16 hours, cooled, and the resulting solid filtered, washed with toluene and dried to give 2-(2′-carboxybenzoyl)-5-diethylaminophenol in 70% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06169185A |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-6101d14e85e44ff5aac0ecc59b3cd271 |
| 出典メモ | uspto-grants-2001_01 |