化工社化工社 化学情報印刷レポート · 研究参考用
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxybenzenethiol | HCID 12765 | — |
| 反応物 | Ethyl 2-bromoheptanoate | HCID 95333 | — |
| 生成物 | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester | HCID 54357246 | 108.8% |
反応手順
2-(4-Methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (13.8 g, 98%) was prepared according to the general method as outlined in example 1 starting from ethyl 2-bromoheptanoate (11 g, 47 mmol) and 4-methoxythiophenol (6 g, 42.8 mmol), as a yellow oil; MS: 297.2 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06172057B2 |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-a53a1964600640f78d7b0b70da2f559b |
| 出典メモ | uspto-grants-2001_01 |