反応式
Br[CH:2]([CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[C:3]([O:5][CH2:6][CH3:7])=[O:4].[CH3:13][O:14][C:15]1[CH:20]=[CH:19][C:18]([SH:21])=[CH:17][CH:16]=1>>[CH2:6]([O:5][C:3](=[O:4])[CH:2]([S:21][C:18]1[CH:19]=[CH:20][C:15]([O:14][CH3:13])=[CH:16][CH:17]=1)[CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[CH3:7]参加物
3
実験手順
2-(4-Methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (13.8 g, 98%) was prepared according to the general method as outlined in example 1 starting from ethyl 2-bromoheptanoate (11 g, 47 mmol) and 4-methoxythiophenol (6 g, 42.8 mmol), as a yellow oil; MS: 297.2 (M+H)+.
出典と根拠
- ORDレコード
- ord-a53a1964600640f78d7b0b70da2f559b
- 出典データセット
- uspto-grants-2001_01
- 特許番号
- US06172057B2
関連ノート
読み込み中…