化工社化工社 化学情報印刷レポート · 研究参考用
4-Decanone → tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Decanone | HCID 12203 | — |
| 反応物 | tert-Butyl carbazate | HCID 70091 | — |
| 溶媒 | Cyclohexane heptane | HCID 21477393 | — |
| 生成物 | tert-Butyl N'-(1-propyl-heptylidene)-hydrazinecarboxylate | HCID 72599202 | 93% |
反応手順
24.76 g (158 mmol) of 4-decanone and 20.94 g (158 mmol) of tert-butyl carbazate are heated for 90 minutes at 80° C. in 250 ml of cyclohexane/heptane mixture (1:1). After cooling, 39.71 g (93%) of a white solid are obtained by crystallization.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06174884B1 |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-37087aa4fed64276a09e56a8bf9701c7 |
| 出典メモ | uspto-grants-2001_01 |