関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Tetrahydrophthalic anhydride | HCID 6810 | — |
| 反応物 | Octadecylamine | HCID 15793 | — |
| 生成物 | HCID 21266144 | HCID 21266144 | 98.7% |
反応手順
Octadecylamine (5.31 g) was added to 4,7,3a,7a-tetrahydroisobenzofuran-1,3-dione (3.00 g). After being stirred for 2 hours at 110° C., the reaction mixture was purified by silica gel column chromatography (silica gel 80 g, chloroform), thereby yielding the entitled compound (7.85 g) as yellow crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06174885B1 |
|---|
| 出典データセット | uspto-grants-2001_01 |
|---|
| ORD ID | ord-ad23ef1d4f0946fd99ee776370455660 |
|---|
| 出典メモ | uspto-grants-2001_01 |
|---|
