化工社化工社 化学情報印刷レポート · 研究参考用
Benzyloxyamine hydrochloride → 2-Benzyloxy-5-bromo-benzo[de]isoquinoline-1,3-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzyloxyamine hydrochloride | HCID 102312 | — |
| 反応物 | 5-Bromobenzo[de]isochromene-1,3-dione | HCID 3907491 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | 2-Benzyloxy-5-bromo-benzo[de]isoquinoline-1,3-dione | HCID 22623899 | 89.1% |
反応手順
O-Benzyl hydroxylamine hydrochloride (0.9 g, 5.6 mmol) and 3-bromo-1,8-naphthalic anhydride (1.3 g, 4.7 mmol, from Example N) were reacted in pyridine (30 mL) following the procedure of Example D to give 1.6 g of the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06177423B1 |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-03ec6581c64c40e6a9e19c9659ee0cf9 |
| 出典メモ | uspto-grants-2001_01 |