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1-Isocyanato-2-phenylbenzene → N-(2-hydroxy-4-trifluoromethylphenyl) N'-(2-phenylphenyl)urea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Isocyanato-2-phenylbenzene | HCID 222280 | — |
| 反応物 | 2-Amino-5-(trifluoromethyl)phenol | HCID 15524277 | — |
| 生成物 | N-(2-hydroxy-4-trifluoromethylphenyl) N'-(2-phenylphenyl)urea | HCID 22011313 | 64% |
反応手順
The urea was prepared from 2-hydroxy 4-trifluoromethyl aniline(example 7a, 0.171 g, 1 mmol)) and 2-phenylphenylisocyanate by general Method B. It was purified by dilution with methylene chloride and precipitation with hexane. Filtering afforded the desired compound(0.24 g, 64%). EI-MS m/z 373(M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06180675B2 |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-1386d8b51b45456d8c24c4c18e451577 |
| 出典メモ | uspto-grants-2001_01 |