化工社化工社 化学情報印刷レポート · 研究参考用
Morpholine → 1,3-Di-cyclopropylmethyl-8-morpholino Xanthine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Morpholine | HCID 8083 | — |
| 反応物 | 1,3-Di-cyclopropylmethyl-8-chloroxanthine | HCID 9814657 | — |
| 生成物 | 1,3-Di-cyclopropylmethyl-8-morpholino Xanthine | HCID 9946149 | — |
反応手順
1,3-Di-cyclopropylmethyl-8-morpholino xanthine was prepared from 1,3-di-cyclopropylmethyl-8-chloroxanthine (0.3 g, 0.001 mol) and morpholine (0.2 g, 0.0022 mol) using an analogous procedure to that described in Example 19. The title product was obtained as a crystalline solid, m.pt. >250° C., yield 0.09 g (26%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06180791B2 |
| 出典データセット | uspto-grants-2001_01 |
| ORD ID | ord-a5dccdb5271345d1beb37992d0f6c3f0 |
| 出典メモ | uspto-grants-2001_01 |