Hydrochloric Acid → HCID 178478516、化合物
反応式
[N:1]1([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH2:14])[CH:5]=[CH:4][N:3]=[CH:2]1.I.CS[C:18]1[C:26]2[CH:27]=[CH:28][CH:29]=[C:24]3[C:25]=2[C:20](=[CH:21][CH:22]=[CH:23]3)[N:19]=1.[ClH:30]>C(O)C>[ClH:30].[ClH:30].[N:1]1([CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][NH:14][C:18]2[C:26]3[CH:27]=[CH:28][CH:29]=[C:24]4[C:25]=3[C:20](=[CH:21][CH:22]=[CH:23]4)[N:19]=2)[CH:5]=[CH:4][N:3]=[CH:2]1参加物
5
実験手順
A mixture of 2.1 g of 8-(1H-imidazol-1-yl)octanamine, 400 ml of ethanol, and 3.2 g of 2-(methylthio)benz[cd]indole hydroiodide was reacted as described in Example 19, giving the base derivative which was then treated with hydrochloric acid giving 1.3 g of the desired hydrochloride salt, mp 222°-224° C.