化工社化工社 化学情報印刷レポート · 研究参考用
Diethylamine → N,N-diethyl-4-iodobenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethylamine | HCID 8021 | — |
| 反応物 | 4-Iodobenzoyl chloride | HCID 74373 | — |
| 溶媒 | Triethylamine | HCID 8471 | — |
| 生成物 | N,N-diethyl-4-iodobenzamide | HCID 875218 | 89.7% |
反応手順
4-Iodobenzoyl chloride (10.0 g) was added portionwise to diethylamine (2.92 g) in triethylamine (40 ml) at 20°. The resulting slurry was stirred at room temperature for 1 h, diluted with ER (150 ml), filtered and evaporated to give the title compound as an orange solid (10.2 g) m.p. 68°-70°.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04730008 |
| 出典データセット | uspto-grants-1988_03 |
| ORD ID | ord-887f5a3b3710439bad711194767794ab |
| 出典メモ | uspto-grants-1988_03 |